CHEM 8M

Summer ’17 content below. Winter content to be updated near the end of fall quarter.

CHEM 8M Syllabus & Schedule SS17

108M Sample Notebook           Sample Experimental Methods

Khan Academy NMR Tutorials (Playlist)

Lectures available via webcast.

DAY 1 – see also “Preparing for the First Day” tab above

Students are responsible for bringing the 8L intro packet to the first day of lab.  Be on-time (15+ min late = dropped from class) and dressed for lab, even though you will not be performing an experiment. You can get a head start on the writing activity, but the error and safety activities require you to be in the lab. If you have taken CHEM 8L (or 108L) in the past, you can bring the completed worksheets from that class, assuming you’ve held onto them! Parts D & E are new and will be provided in the lab.

8M Technical Writing – A-C – bring your own

8M Technical Writing – D-E – provided in lab

**Do not come to lab unless you are enrolled. If you are added to the class (from the wait-list or otherwise) after the first lab meeting, please contact me (cambinde@ucsc.edu) ASAP.

EXPERIMENTS – summer ’17 material below

Exp 1 – Separation of Carvone and Limonene

Exp 2 – Isolation of Excedrin Components EtOAc

Exp 3 – Oxidation of Benzhydrol

Exp 4 – Colorful Chemistry

Exp 5 – Preparation of Fruity Fragrances

IR Hexanol and Acetic Acid       IR Isoamyl Alcohol and Acetic Acid

Exp 6 – Synthesis of Aspirin – Exam Prep

LECTURE HANDOUTS (copies provided in class) – these are supplements to lecture, NOT lecture notes!

Lecture 1 – Column Chromatography

Lecture 2 – Excedrin Flow Chart

Lecture 3 – NMR Tables

Lecture 3/4 – 1H NMR of Benzhydrol & Benzophenone

Lecture 5 – Dyes & Fibers

Lecture 6/7 – 1H NMR Analysis of Esters

Lecture 8 – 1H NMR of Aromatics (Aspirin)

Lecture 9 – 13C NMR & IR – Aspirin